鍏充簬鎴戜滑
鍔犲叆鏀惰棌
姝ョ惁瀹為獙瀹よ澶囪锤鏄擄紙涓婃捣锛夋湁闄愬叕鍙伏/p>
4 骞滁/span>
鐧介噾浼氬憳
鐧介噾浼氬憳
宸茶璇?/p>
鎷ㄦ墦鐢佃瘽
鑾峰彇搴曚环
鎻愪氦鍚庯紝鍟嗗灏嗘淳浠ｈ〃涓烘偍涓撲汉鏈嶅姟
姝ョ惁瀹為獙瀹よ澶囪锤鏄擄紙涓婃捣锛夋湁闄愬叕鍙伏/p>
鐧介噾浼氬憳
宸茶璇?/p>
鍦熷￥涓湁鏈烘隘妫€娴嬬殑鏂规硶楠岃瘉
鏈夋満姘被鍐滆嵂鏄惈姘厓绱犵殑鏈夋満鍖栧悎鐗╋紝鏇惧箍娉涚敤浜庨槻娌绘鐗╃梾銆佽櫕瀹崇瓑锛屼富瑕佸垎涓轰互鑻负鍘熸枡鍜屼互鐜垔浜岀儻涓哄師鏂欑殑涓ゅぇ绫汇€傚叾鍖栧鎬ц川绋冲畾銆侀毦鍒嗚В銆佹槗娈嬬暀锛屾寔缁牬鍧忕潃鐢熸€佺幆澧冿紝涓斿叾鐢熺墿姣掓€у拰鑷寸檶鎬э紝涓ラ噸褰卞搷浜虹被鍋ュ悍锛岀幇宸查€愭笎绂佹鎴栧噺灏戜娇鐢ㄣ€侟/p>
鏈簲鐢ㄦ牴鎹幆澧冩爣鍑 HJ 783-2016銆丠J 921-2017 绛夛紝灏嗘牱鍝佸埄鐢ㄦ鐞︿竴绔欏紡鍦熷￥鍒嗘瀽鏂规鐨勮悆鍙栦华銆佸畾閲忔祿缂╀华澶勭悊鍚庯紝杩涜 GC 鍒嗘瀽浠ユ娴嬫湁鏈烘隘鍖栧悎鐗╅噷 8 缁勫垎鐨勫洖鏀剁巼锛屾暣涓祦绋嬪湪 1 灏忔椂鍐呭畬鎴愶紝鍚屾椂涓€娆″钩琛岃悆鍙 6 涓牱鍝侊紝鑰冨療鏇村叿浠ｈ〃鎬у拰涓ヨ皑鎬э紝澶уぇ鎻愰珮浜嗗伐浣滄晥鐜囷紝涔熶紭鍖栦簡浼犵粺璐规椂鐨勬牱鍝佸鐞嗗拰绻佺悙鐨勬搷浣滄祦绋嬨€侟/p>
1
璁惧
蹇€熸憾鍓傝悆鍙 SpeedExtractor庐E-916
瀹氶噺娴撶缉浠 Syncore庐R-12+鍥炴祦妯″潡
GC Agilent 7890A+7693 Autosampler
鈻蹇€熸憾鍓傝悆鍙栦华 E-916
2
鑽搧鍙婅€楁潗
鏈夋満姘爣鍑嗗搧锛?00 g/mL锛堻/p>
璐ㄦ帶鍦燂紙瑗挎牸鐜涳級
纭呰椈鍦燂細绮掑緞 30-40 鐩?/p>
鐭宠嫳鐮傦細绮掑緞 25-50 鐩?/p>
涓欓叜锛氬啘娈嬬骇
姝ｅ繁鐑凤細鍐滄畫绾?/p>
3
瀹為獙鏂规硶
1銆佹鐞︽牱鍝佺灏剧瀹氬鍑嗙‘搴﹁€冨療
涓轰簡鑰冨療鏍峰搧绠″畾瀹圭殑鍑嗙‘鎬э紝灏嗘牱鍝佹憾娑插垎鍒敤 1mL 灏剧鍜 1mL 瀹归噺鐡跺畾瀹癸紝骞惰繘琛屽惈閲忔祴瀹氥€侟/p>
2銆佸揩閫熸憾鍓傝悆鍙栦华鍥炴敹鐜囪€冨療
鍏堣繘琛岃悆鍙栨睜鏍峰搧瑁呭～锛氱煶鑻辩爞-纭呰椈鍦?鏍峰搧-鐭宠嫳鐮傦紝鍩鸿川骞抽潰涓庢睜瀛愰《绔鐣 1cm 宸﹀彸鐨勭┖闅欍€傜劧鍚庡皢钀冨彇姹犵珛鍗虫斁鍏ュ凡棰勭儹濂界殑浠櫒涓紝寮€濮嬭悆鍙栥€侟span style="text-decoration-line: underline; box-sizing: border-box;">钀冨彇鏂规硶濡備笅锛欬/strong>
琛?锛氬揩閫熸憾鍓傝悆鍙栦华 E-916 钀冨彇鍙傛暟
|
钀冨彇娓╁害 |
100 鈩傸/p> |
|
鍘嬪姏 |
100 bar |
|
钀冨彇姹燑/p> |
40 mL |
|
鎺ユ敹鐡迭/p> |
150 mL |
|
婧跺墏 |
涓欓叜/姝ｅ繁鐑凤細50%/50% |
|
寰幆 |
2 |
|
棰勭儹 |
榛樿 |
|
淇濇寔 |
10/10 min |
|
鎺掓恫 |
2 /2min |
|
婧跺墏鍐插埛 |
2 min |
|
姘斾綋鍐插埛 |
2 min |
3銆佸畾閲忔祿缂╀华 Syncore庐R-12 鍥炴敹鐜囪€冨療
鍦 60mL 鐨勪笝閰?姝ｅ繁鐑凤紙1锛?锛夋憾娑蹭腑鍔犲叆鏈夋満姘殑鏍囧噯婧舵恫10渭L锛岀敤瀹氶噺娴撶缉浠 R-12 杩涜娴撶缉锛屽苟鐢ㄦ宸辩兎缃崲婧舵恫涓ゆ锛屾瘡娆＄害 2mL銆傚湪绗 2 娆＄疆鎹㈠悗灏嗘憾娑叉祿缂╄嚦 1mL 宸﹀彸鍚庯紝鐢ㄦ宸辩兎瀹氬鍒 1mL锛屽緟涓婃満鍒嗘瀽妫€娴嬨€侟/p>
鈻瀹氶噺娴撶缉浠 Syncore庐R-12
4銆佽川鎺у湡鏍风殑瀹為獙鑰冨療
鑰冨療涓や釜璐ㄦ帶鍦熸牱鐨勬儏鍐碉紝鍒嗗埆灏嗗湡鏍疯濉繘钀冨彇姹犲悗锛岀敤 E-916 杩涜钀冨彇锛屽甫灏剧鐨 150mL 鏍峰搧绠℃帴鏀跺ソ钀冨彇娑插悗锛岀洿鎺ヨ浆绉昏嚦 R-12 涓繘琛屾祿缂╋紝骞剁粡涓ゆ婧跺墏缃崲锛屾祿缂╄嚦绾 1mL锛屽畾瀹瑰緟娴嬨€侟/p>
4
瀹為獙缁撴灉
1銆佸熬绠″畾瀹瑰疄楠岀粨鏋淈/span>
鏍峰搧绠″畾瀹 1mL 鍜屽閲忓畾瀹圭殑缁撴灉姣旇緝濡侟span style="text-decoration-line: underline; box-sizing: border-box;">琛 2銆侟/p>
琛?锛氬熬绠″畾瀹规祴璇曠粨鏋淈/span>
|
|
瀹归噺鐡跺畾瀹瑰惈閲廃/p> |
鏍峰搧绠″畾瀹瑰惈閲廃/p> |
|
伪-666 |
190.60 |
190.46 |
|
尾-666 |
186.56 |
186.83 |
|
纬-666 |
192.36 |
192.33 |
|
未-666 |
184.80 |
185.67 |
|
p,p锛?DDE |
205.90 |
206.14 |
|
p,p锛?DDD |
216.10 |
216.39 |
|
o,p -DDT |
213.37 |
213.83 |
|
p,p锛?DDT |
203.53 |
203.31 |
鐢变笂琛ㄥ彲鐭ワ紝鐢辨鐞︽牱鍝佺瀹氬鍒嗘瀽鐨勬暟鎹笌瀹归噺鐡跺畾瀹瑰熀鏈棤宸埆锛岃鏄庣洿鎺ョ敤鏍峰搧绠″畾瀹圭殑鏂规硶鍙锛屼笖閬垮厤浜嗚浆绉诲畾瀹规椂閫犳垚鐨勬牱鍝佹崯澶便€侟/p>
2銆佸揩閫熸憾鍓傝悆鍙栦华瀹為獙缁撴灉
鑰冨療骞宠钀冨彇鐨勫钩琛屾€у拰鍥炴敹鐜囥€侟span style="text-decoration-line: underline; box-sizing: border-box;">缁撴灉瑙佷笅琛細
琛?锛氬湡澹や腑鏈夋満姘殑娴嬪畾缁撴灉
|
鍥炴敹鐜嘃/p> |
1 |
2 |
3 |
4 |
5 |
|
伪-666 |
96.6% |
99.0% |
98.8% |
99.4% |
98.6% |
|
尾-666 |
102.9% |
105.3% |
105.2% |
106.2% |
105.9% |
|
纬-666 |
97.9% |
100.0% |
100.0% |
100.6% |
99.8% |
|
未-666 |
95.1% |
96.5% |
94.6% |
95.9% |
90.5% |
|
p,p锛?DDE |
100.9% |
104.0% |
103.7% |
105.3% |
104.6% |
|
p,p锛?DDD |
105.5% |
108.8% |
108.7% |
110.0% |
109.0% |
|
o,p -DDT |
94.1% |
92.7% |
93.9% |
92.8% |
93.7% |
|
p,p锛?DDT |
95.6% |
93.6% |
95.8% |
94.4% |
94.3% |
鐢辫〃 3 鍙煡锛? 涓钩琛屾牱鐨勬瘡涓粍鍒嗗洖鏀剁巼鍧囧湪鍏佽鐨 RSD 鑼冨洿鍐呫€備笖鍥炴敹鐜囧潎鍦 90% 浠ヤ笂锛岃鏄庡揩閫熸憾鍓傝悆鍙栫殑绮惧瘑搴︾鍚堣姹傘€佽悆鍙栨柟娉曞悎鐞嗐€侟/p>
3銆佸畾閲忔祿缂╀华瀹氶噺娴撶缉瀹為獙缁撴灉
骞宠澶勭悊 6 涓牱鍝侊紝鑰冨療瀹氶噺娴撶缉鐨勭粨鏋滅ǔ瀹氭€у拰鍑嗙‘鎬э紝缁撴灉濡傝〃 4銆侟/strong>
琛?锛氬湡澹や腑鏈夋満姘殑娴嬪畾缁撴灉
|
鍥炴敹鐜嘃/p> |
1 |
2 |
3 |
4 |
5 |
6 |
|
伪-666 |
89.6% |
94.3% |
88.4% |
93.4% |
98.5% |
94.5% |
|
尾-666 |
92.9% |
97.9% |
97.0% |
102.8% |
97.5% |
101.4% |
|
纬-666 |
88.9% |
93.5% |
91.0% |
96.9% |
96.2% |
97.3% |
|
未-666 |
92.1% |
96.7% |
96.8% |
103.0% |
95.9% |
100.2% |
|
p,p锛?DDE |
93.6% |
98.0% |
97.3% |
102.9% |
97.1% |
101.0% |
|
p,p锛?DDD |
90.5% |
94.6% |
95.0% |
100.4% |
94.6% |
97.2% |
|
o,p -DDT |
98.8% |
104.8% |
104.7% |
110.9% |
104.0% |
108.6% |
|
p,p锛?DDT |
101.0% |
107.7% |
106.9% |
114.4% |
106.2% |
112.0% |
鏈変笂琛ㄥ彲鐭ワ紝浣庢哺鐐圭粍鍒嗙殑 666 鍥炴敹鐜囧彲浠ヨ揪鍒 90% 鍙婁互涓婏紝涓 6 涓暟鎹钩琛屾€т篃鍦ㄥ悎鐞嗚寖鍥村唴锛岃鏄庢鐞﹀畾閲忔祿缂╀华閰嶄笂鍥炴祦妯″潡鑳芥彁楂樻牱鍝佸洖鏀剁巼鍜屾暟鎹ǔ瀹氭€с€侟/p>
4銆佽川鎺у湡瀹為獙缁撴灉
閫夊彇 2 涓壒娆¤川鎺у湡杩涜鍏ㄦ祦绋嬭€冨療楠岃瘉锛屽緱鍒扮粨鏋滀笅琛細
琛?锛氳川鎺у湡鐨勬祴瀹氱粨鏋淈/span>
|
|
ZK1 娴嬮噺鍊稽/p> |
鑼冨洿 |
ZK2 娴嬮噺鍊稽/p> |
鑼冨洿 |
|
伪-666 |
170.33 |
98-228 |
196.18 |
120-387 |
|
尾-666 |
186.4 |
99-231 |
208.04 |
120-386 |
|
纬-666 |
182.06 |
99-232 |
200.88 |
120-387 |
|
未-666 |
182.16 |
99-231 |
204.44 |
120-387 |
|
p,p锛?DDE |
116.53 |
64-149 |
163.95 |
96-310 |
|
p,p锛?DDD |
113.87 |
64-149 |
155.36 |
96-309 |
|
o,p -DDT |
108.19 |
63-147 |
150.3 |
96-310 |
|
p,p锛?DDT |
88.09 |
64-149 |
133.06 |
96-309 |
鏈夎〃 5 鍙煡锛屼袱涓川鎺у湡鐨勫惈閲忓潎鍦ㄨ川鎺ц寖鍥村唴锛岃鏄庢暣涓悆鍙?娴撶缉鏂规硶鍙銆傚彲椤哄埄杩涜鍚庣画鏍峰搧鐨勬娴嬪垎鏋愩€侟/p>
5
缁撹
鏈柟娉曚娇鐢ㄥ揩閫熸憾鍓傝悆鍙栦华 E-916锛屽埄鐢ㄩ珮娓╅珮鍘嬬殑钀冨彇鍘熺悊锛岃幏寰楃殑瀹為獙缁撴灉绗﹀悎瑕佹眰锛屽悓鏃朵竴娆″钩琛岃悆鍙 6 涓紝绾 30min 瀹屾垚涓€鎵癸紝澶уぇ鎻愰珮浜嗚悆鍙栨晥鐜囷紝绠€鍖栦簡鏍峰搧鍓嶅鐞嗙殑绛夊緟鏃堕棿锛屽鍔犳牱鍝侀€氶噺銆侟/p>
鍚屾椂钀冨彇娑叉帴鏀剁摱鍙互鏃犵紳杞Щ鑷冲畾閲忔祿缂╀华涓婅繘琛屾憾鍓傛祿缂╁畾瀹癸紝鍑忓皯鏍峰搧杞Щ閫犳垚鐨勬崯澶憋紝纭繚浜嗘湁鏈虹墿鐨勯珮鍥炴敹鐜囧拰缁撴灉绋冲畾鎬с€侟/p>
6
鍙傝€冩枃鐚?/strong>
HJ 783-2016 鍦熷￥鍜屾矇绉墿鏈夋満鐗╃殑鎻愬彇鍔犲帇娴佷綋钀冨彇娉曘€侟/p>
HJ 921-2017 鍦熷￥鍜屾矇绉墿鏈夋満姘啘鑽殑娴嬪畾姘旂浉鑹茶氨娉曘€侟/p>
SpeedExtractor庐E-916 Operation Manual.
Syncore庐Platform Operation Manual.
闀挎寜涓婃柟浜岀淮鐮佽仈绯绘垜浠?/strong>
鎴栨嫧鎵撹仈绯荤數璇濓細
400 - 880 - 8720
寰俊鍏紬鍙饵/strong>
姝ョ惁鏅烘収瀹為獙瀹｜/span>
娣樺疂瀹樻柟鏃楄埌搴?nbsp;
鐟炲＋姝ョ惁
鎵嬫満鐗堬細
涓婁竴绡嘃/a>
