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<h3><strong><span>概念</span></strong><strong></strong></h3><p><span>水热合成反应釜又称聚合反应釜、高压消解罐、水热反应釜、压力溶弹、消化罐</span>.<span>是利用罐体内强酸或强碱且高温高压密闭的环境来达到快速消解难溶物质的目的、�/span></p><h3><strong><span>水热合成反应釜是一种能分解难溶物质的密闭容器。可用于原子吸收光谱及等离子发射等分析中的溶样预处理；也可用于小剂量的合成反应；还可利用罐体内强酸或强碱且高温高压密闭的环境来达到快速消解难溶物质的目的。在气相、液相、等离子光谱质谱、原子吸收和原子荧光等化学分析方法中做样品前处理。是测定微量元素及痕量元素时消解样品的得力助手、�/span></strong><strong></strong></h3><p><span>可在铅、铜、镉、锌、钙、锰、铁、汞等重金属测定中应用，还可作为一种耐高温耐高压防腐高纯的反应容器，以及有机合成、水热合成、晶体生长或样品消解萃取等方面。在样品前处理消解重金属、农残、食品、淤泥、稀土、水产品、有机物等。因此，在石油化工、生物医学、材料科学、地质化学、环境科学、食品科学、商品检验等部门的研究和生产中被广泛使用、�/span></p><p><span>特点</span></p><p><span>1<span>� 抗腐蚀性好，无有害物质溢出，减少污染，使用安全、�/span></p><p><span>2<span>� 升温、升压后，能快速无损地溶解在常规条件下难以溶解的试样及含有挥发性元素的试样、�/span></p><p><span>3<span>� 外观美观，结构合理，操作简单，缩短分析时间，数据可靠、�/span></p><p><span>4<span>� 内有聚四氟乙烯衬套，生成护理，可耐酸，碱等、�/span></p><p><span>5<span>、不锈钢上盖和内胆上盖设有防爆孔，超压可通过防爆孔自动泄厊�/span></p><p><span>6</span><span>�?/span><span>可替代铂坩埚解决高纯氧化铝中微量元素分析的溶样处理问题。烘箱中使用的高压消解罐，也称为溶样器、压力溶弹、水热合成反应釜、消化罐、聚四氟乙烯高压罐，是测定微量元素及痕量元素时消解样品的得力助手。样品前处理消解重金属、农残、食品、淤泥、稀土、水产品、有机物等、�/span></p><h2><strong><span>操作方法</span></strong><strong></strong></h2><h2><strong><span>1<span>�?/span></strong><strong><span>将反应物倒入聚四氟乙烯衬套或</span>PPL<span>衬套内，并保证加料系数小亍�/span><span>0.8</span><span>、�/span></strong><strong></strong></h2><p><span>2<span>�?/span><span>确保釜体下垫片位置正确，然后放入聚四氟乙烯衬套或</span>PPL<span>衬套和上垫片，先拧紧釜盖，然后用</span><span>加力</span><span>杆把釜盖旋扭拧紧为止、�/span></p><p><span>3<span>�?/span><span>将水热合成反应釜置于加热器内，按照规定的升温速率升温至所需反应温度、�/span>(<span>小于规定的安全使用温�?/span><span>)</span><span>、�/span></p><p><span>4<span>�?/span><span>当确认腹内温度低于反应物系种溶剂沸点后方能打开釜盖进行后续操作。待反应结束将其降温时，也要严格按照规定的降温速率操作，以利安全和反应釜的使用寿命、�/span></p><p><span>5<span>�?/span><span>确认釜内温度低于反应物系种溶剂沸点后，先�?/span><span>加力杅�/span><span>把釜盖旋扭松开，然后将釜盖打开、�/span></p><p><span>6<span>�?/span><span>水热合成反应釜每次使用后要及时将其清洗干净，以免锈蚀。釜体、釜盖线密封处要格外注意清洗干净，并严防将其碰伤损坏、�/span></p><p><span>材质</span></p><h2><strong><span>⑟�span>釜体</span></strong><strong><span>采用锻速�/span></strong><strong><span>304<span>优质不锈钢，采用圆形榫槽密封</span><span>＋�/span><span>手动螺旋坚固</span><span>.</span><span>具有密封性好</span><span>＋�/span><span>安全系数髗�/span><span>＋�/span><span>消耗酸溶剂尐�/span><span>＋�/span><span>使用简便！</span></strong><strong></strong></h2><p><span>内胆材质为聚四氟乙烯</span>(PTFE<span>简�?/span><span>F4)</span><span>，其特性：</span></p><p><span>1.<span>耐高温：使用温度</span><span>-200</span><span>｝�/span><span>+2</span><span>4</span><span>0ℂ�span>：�/span></p><p><span>2.<span>耐低温：</span><span>-196ℂ�/span><span>可保�?/span><span>5%</span><span>：�/span></p><p><span>3.<span>耐腐蚀：耐强酸、强碱、王水和各种有机溶剂：�/span></p><p><span>4.<span>内胆上盖设有防爆孓�/span></p><p><span>5</span><span>.<span>耐绝缘：介电性能与温度、频率无关；</span></p><p><span>6</span><span>.<span>高润滑：固体材料中摩擦系数低：�/span></p><p><span>7</span><span>.<span>不粘附：不粘附任何物质；自润性强：固体材料中摩擦系数丹�/span><span>0.04</span></p><p><span>8</span><span>.<span>无毒害：具有生理惰性，可植入人体内；耐老化可长期在大气中使�?/span></p><p><span>9</span><span>.<span>防污染：金属元素空白值低，铅含量小于</span><span>10-11 g/ml</span><span>，铀含量小于</span><span>10-12 g/ml</span><span>：�/span></p><p><span>10</span><span>.<span>防泄漏：从离�?/span><span>1.2</span><span>米高处落下，瓶体不破裂，瓶盖不脱落，无破损泄漏现象、�/span></p><p><strong><span>①�span>对位聚苯水热合成反应釛�/span></strong><strong></strong></p><p><span>对位聚苯材质</span><span>耐高温：使用温度</span>-200<span>｝�/span><span>+2</span><span>6</span><span>0ℂ�/span></p><p><span>经高温烧结冷却而制戏�/span><span>耐强酸强碱、王水有机溶剁�/span></p><p><span>性能</span><span>优于聚四氟乙烯制�?/span><span>耐高温性能方面表现更优弁�/span></p><p><span>工艺</span><span>深棕色、表面无裂纹</span><span>外形美观</span></p><table cellspacing="0" cellpadding="2" border="1" bordercolor="#f2f2f2" width="100%"><tbody><tr><td><p><span>规格</span></p></td><td><p><span>PF-25ML</span></p></td><td><p><span>PF-50ML</span></p></td><td><p><span>PF-100ML</span></p></td><td><p><span>PF-150ML</span></p></td><td><p><span>PF-200ML</span></p></td><td><p><span>PF-300ML</span></p></td><td><p><span>PF-350ML</span></p></td><td><p><span>PF-400ML</span></p></td><td><p><span>PF-500ML</span></p></td><td><p><span>PF-1L</span></p></td></tr><tr><td><p><span>容量</span></p></td><td><p><span>25ML</span></p></td><td><p><span>50ML</span></p></td><td><p><span>100ML</span></p></td><td><p><span>150ML</span></p></td><td><p><span>200ML</span></p></td><td><p><span>300ML</span></p></td><td><p><span>350ML</span></p></td><td><p><span>400ML</span></p></td><td><p><span>500ML</span></p></td><td><p><span>1L</span></p></td></tr><tr><td><p><span>材质</span></p></td><td colspan="10"><p><span>优质锻速�span>304</span><span>材质，可搭配聚四氟乙烯（</span><span>PTFE</span><span>� 内衬或者对位聚�?/span><span>(PPL)</span></p></td></tr><tr><td><p><span>压力</span></p></td><td colspan="10"><p><span>≣�span>6MPA</span></p></td></tr><tr><td><p><span>温度</span></p></td><td colspan="10"><p><span>聚四氟乙烯≤<span>240</span><span>ℂ�/span><span>� </span><span>对位聚苯＇�/span><span>PPL</span><span>）≤</span><span>280</span><span>ℂ�/span></p></td></tr><tr><td><p><span>备注</span></p></td><td colspan="10"><p><span>安全建议盛放液体为内衬体积的三分之一或者三分之事�/span></p></td></tr></tbody></table> </div>  <div class="cxd"> <div class="cxd_tit"><span></span>创新炸�/div> <p style=" color: #333; font-size: 14px; margin: 10px 0 0; line-height: 26px;"> 暂无数据� </p> </div>  <div class="xgfa"> <div class="xgfa_tit"> <div> <span></span>相关方案 </div> </div> <div class="xgfa_box" style="display: block;"><div style="padding:10px;">暂无相关方案、�/div> </div> </div> <script> $(function(){ // 切换 $(".xgfa_tit_ul li").hover(function(){ $(".xgfa_tit_ul li").css({"color":"#4F5862","border-bottom-color":"transparent"}); 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